My position: Material Testing > Atomic Force Microscope AFM
Atomic Force Microscope AFM
Instrument model
Bruker Dimension ICON; Bruker Multimode 8; Oxford MFP 3D infinity; Oxford CypherES, etc.
Service model
Commissioned test
Service cycle
5-8 working days after receiving samples
Service items

Shape observation (2 positions)

$400/Sample

Probe loss

$200/Batch

Make up the difference

Negotiable

Sample

$50
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Testing Description

1.Surface morphology, thickness, and roughness testing of powder, solution, and bulk samples.
2. Surface morphology of biological/fiber samples
3.Phase diagram
4.PFM (piezoelectric force microscope), EFM (electrostatic force microscope), KPFM (surface potential), MFM (magnetic force microscope),
C-AFM/PeakForce TUNA (conductive force microscope), Young’s modulus/modulus distribution, force Special modes such as curve, submerged, and variable temperature.
For more test requirements, please feel free to contact us

Sample requirements

1. Sample status: it can be powder, block, film sample;
2. Powder samples: The particles are generally no more than 5 microns, 20mg is provided, and the liquid is no less than 1ml. If the size is too large, please con-sult the customer manager in advance;
3. For powderliquid samples, please note the sample preparation conditions, including dispersion, ultrasonic time and preparation concentration;
4. Film or block sample size requirements: length and width between 0. 53cm, thickness between 0.1-1cm, surface roughness no more than 5um, be sure to mark the test surface!
5. For testing piezoelectric and surface potential materials, samples need to be prepared on a conductive substrate, the size of which is larger than 0.5*0.5cm.
For other questions, please consult your account manager.

Examples

The form of the results of different models of instruments will be different. The following shows the results of Bruker Dimension ICON model AFM, for reference only.

1. Surface morphology and surface roughness AFM can study the sample surface morphology, nanostructure, chain conformation, etc., and obtain information such as nanoparticle size, pore size, material surface roughness, material surface defects, etc. conditions change). The topography of the sample can also be displayed in a rich three-dimensional simulation, making the image more suitable for human intuitive vision. The figure below characterizes the 2D geometry, 3D height and roughness of the nanoparticles.

2. Precise positioning such as: nanosheet thickness/step height What is precise positioning? Just need to spend a little time to find this place. Measurement of high aspect ratio structures, such as trenches and steps, is often required during semiconductor processing to determine the depth and width of the etch. These can only be measured by cutting the sample along the cross section under SEM, and AFM can measure it non-destructively. The resolution of AFM in the vertical direction is about 0.1 nm, so it can be well used to characterize the thickness of nanosheets. The figure below characterizes the step height and nanosheet thickness map.

3. Phase diagram As an important extension of the tapping mode, the phase mode is determined by detecting the difference between the phase angle of the signal source driving the vibration of the micro-cantilever probe and the phase angle of the actual vibration of the micro-cantilever probe (ie, the phase shift of the two). change to image. There are many factors that cause this phase shift, such as sample composition, hardness, viscoelastic properties, modulus, etc. To put it simply, if the contrast between the two materials is relatively small in terms of AFM morphology, but you really want to explain what kind of film this is on, you can use the two-dimensional topography map + phase map to Description (provided that the physical properties of the two materials are relatively different, and the phase diagram has obvious contrast signals).

The test raw files of Bruker AFM instruments in .spm format can be opened with the Bruker offline software Nanoscope analysis software.

FAQs

1. Why should the particle or surface roughness of the AFM test sample not be too large?
Generally speaking, the Z-phase range tested by AFM instruments is about 10um (some instruments may only have 2um), so samples with excessive surface fluctuations may exceed the scanning range of the instrument, and samples with relatively large roughness may cause the needle tip to be blunt or blunt. Contamination has a great impact on image quality, and wear and tear cannot be repaired increasing the cost of consumables.
2. AFM cannot capture the desired effect, and the surface morphology or roughness does not meet your expectations?
AFM shooting also needs to constantly find a suitable position to shoot. The surface morphology and roughness of different shooting parts of the same sample are very likely to be inconsistent, because the imaging range of the atomic force microscope is small, which is closely related to whether the surface of the sample is uniform.
3. Can AFM be measured if the sample has poor conductivity? Need gold spray treatment?
AFM routine test items have no requirements on the conductivity of the sample, and non-conductive samples can also be tested without gold spray treatment, but the test of some electrical modules, such as KPFM, requires the sample to be conductive, and the gold particles have a certain size Yes, gold spraying may affect the morphology, so gold spraying is generally not recommended.
4. How to get the roughness of the sample from the AFM results?
Surface roughness calculation, which is the advantage of AFM, can get the roughness of the whole image and the roughness of the selected area, Rq: root mean square roughness and Ra: average roughness, both of which can be referenced when using Just keep the same data set. If you need to get the roughness value, select the height map in the offline software of AFM, and click roughness directly.

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